(S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

Base Information

Chemical Name:(S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid
CAS No.:88636-11-7
Molecular Formula:C₂₅H₂₂N₂O₄
Molecular Weight:414.461
Hs Code.:

Synonyms:(S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

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Chemical Property of (S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

Chemical Property:

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Technology Process of (S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

There total 1 articles about (S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 73-22-3,27732-43-0,80206-30-0,27813-82-7
L-Tryptophan

: 74606-98-7,88636-10-6,88636-11-7,88668-83-1,88668-84-2
(S)-2-Benzoylamino-3-(1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

Guidance literature:: DOI:10.1021/ja00536a067

Reference yield:

: 88636-11-7
(S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

: 86749-47-5
C₃₀H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Ac₂O; 2.) AlCl₃ / 1.) 100 deg C, 15 min; 2.) dichloroethane, reflux, 30 min

2: Zn / I₂ / tetrahydrofuran / 14 h / 50 °C

3: NaH / dimethylformamide / 1.33 h / Ambient temperature

With aluminium trichloride; acetic anhydride; sodium hydride; zinc; iodine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja00318a044

Reference yield:

: 88636-11-7
(S)-2-Benzoylamino-3-((S)-1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

: 86783-97-3
C₂₉H₂₄N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Ac₂O; 2.) AlCl₃ / 1.) 100 deg C, 15 min; 2.) dichloroethane, reflux, 30 min

2: Zn / I₂ / tetrahydrofuran / 14 h / 50 °C

With aluminium trichloride; acetic anhydride; zinc; iodine; In tetrahydrofuran;
DOI:10.1021/ja00318a044