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oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(3-)-N,N',N'',N''')technetium(V)

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  • Chemical Name:oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(3-)-N,N',N'',N''')technetium(V)
  • CAS No.:99829-02-4
  • Molecular Formula:C13H25N4O3Tc
  • Molecular Weight:383.274
  • Hs Code.:
oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato<sup>(3-)</sup>-N,N',N'',N''')technetium(V)

Synonyms:oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(3-)-N,N',N'',N''')technetium(V)

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Chemical Property of oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(3-)-N,N',N'',N''')technetium(V)
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Technology Process of oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(3-)-N,N',N'',N''')technetium(V)

There total 1 articles about oxo(3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(3-)-N,N',N'',N''')technetium(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With NaCl; NaHCO3; stannous tartrate; In water; to the ligand in acidic 0,9 % NaCl soln. was added NH4TcO4 and NaHCO3; mixt. overlayered with Et2O, addn. of a suspn. of the Sn salt in 0,9 % NaCl soln., mixt. stirred for 10 min at room temp., aq. soln. extd. with ether; ether exts. were dried (Na2SO4), concd., and chromd. (silicagel, Et2O); Tc complex eluated by MeOH, filtered eluent evapd. to dryness (<25°C); residue dissolved in Et2O, recrystd. at -20°C; crystals washed with cold Et2O and dried in air;
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