N,N'-Bis(3-oximino-2-methyl-2-butyl)-1,3-diaminopropane

Base Information

Chemical Name:N,N'-Bis(3-oximino-2-methyl-2-butyl)-1,3-diaminopropane
CAS No.:17023-02-8
Molecular Formula:C13H28N4O2
Molecular Weight:272.391
Hs Code.:2928000090
European Community (EC) Number:683-454-8
Mol file:17023-02-8.mol

Synonyms:N,N'-BIS(3-OXIMINO-2-METHYL-2-BUTYL)-1,3-DIAMINOPROPANE;SCHEMBL8693325;AKOS024330661

Suppliers and Price of N,N'-Bis(3-oximino-2-methyl-2-butyl)-1,3-diaminopropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N,N'-BIS(3-OXIMINO-2-METHYL-2-BUTYL)-1,3-DIAMINOPROPANE Aldrich
10mg
$ 57.00

Total 1 raw suppliers

Chemical Property of N,N'-Bis(3-oximino-2-methyl-2-butyl)-1,3-diaminopropane

Chemical Property:

Boiling Point:433.0±40.0 °C(Predicted)
PKA:11.83±0.10(Predicted)
PSA：89.24000
Density:1.04±0.1 g/cm3(Predicted)
LogP:2.59490
XLogP3:0.9
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:272.22122615
Heavy Atom Count:19
Complexity:304

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N'-BIS(3-OXIMINO-2-METHYL-2-BUTYL)-1,3-DIAMINOPROPANE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NO)C(C)(C)NCCCNC(C)(C)C(=NO)C
Isomeric SMILES:C/C(=N\O)/C(NCCCNC(/C(=N/O)/C)(C)C)(C)C

Technology Process of N,N'-Bis(3-oximino-2-methyl-2-butyl)-1,3-diaminopropane

There total 3 articles about N,N'-Bis(3-oximino-2-methyl-2-butyl)-1,3-diaminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 4,8-diaza-3,3,9,9-tetramethyl-undeca-2,10-dione

: 17023-02-8
3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioxime

Guidance literature:: With hydroxylamine hydrochloride; In methanol; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85336-9

Reference yield: 40.0%

: 67-56-1
methanol

: 37557-67-8
2-chloro-2-methyl-3-nitrosobutane

: 109-76-2,54018-94-9
Trimethylenediamine

: 15403-10-8
3-methoxy-3-methyl-2-butanone oxime

: 17023-02-8
3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioxime

: 3-(3-aminopropyl)amino-3-methylbutan-2-one

Guidance literature:: 0 deg C -> room temp., then reflux, 6 h;
DOI:10.1016/S0040-4020(01)85336-9

Reference yield:

: 2648-71-7
3-bromo-3-methyl-2-butanone

: 17023-02-8
3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioxime

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

2: 94 percent / hydroxylamine hydrochloride / methanol / 18 h / Ambient temperature

With hydroxylamine hydrochloride; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85336-9