carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

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Chemical Name:carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester
CAS No.:1451073-54-3
Molecular Formula:C₃₀H₂₀N₂O₇S₂
Molecular Weight:584.63
Hs Code.:

Synonyms:carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

There total 3 articles about carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1451073-48-5
1-(4-hydroxymethyl-phenyl)-3,4-bis-phenylsulfanyl-pyrrole-2,5-dione

: 7693-46-1
4-Nitrophenyl chloroformate

: 1451073-54-3
carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1039/c3cc45220d

Reference yield:

: 1442447-57-5
3,4-dibromo-1-(4-hydroxymethyl-phenyl)-pyrrole-2,5-dione

: 1451073-54-3
carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / 20 °C

2: pyridine / dichloromethane / 24 h / 20 °C

With pyridine; triethylamine; In dichloromethane;
DOI:10.1039/c3cc45220d

Reference yield:

: 108-98-5
thiophenol

: 1451073-54-3
carbonic acid 4-(2,5-dioxo-3,4-bis-phenylsulfanyl-2,5-dihydro-pyrrol-1-yl)-benzyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / 20 °C

2: pyridine / dichloromethane / 24 h / 20 °C

With pyridine; triethylamine; In dichloromethane;
DOI:10.1039/c3cc45220d