2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

Base Information

Chemical Name:2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol
CAS No.:882977-67-5
Molecular Formula:C₁₈H₁₈Cl₂N₂OS
Molecular Weight:381.326
Hs Code.:

Synonyms:2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

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Chemical Property of 2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

Chemical Property:

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Technology Process of 2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

There total 4 articles about 2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5348-42-5
4,5-Dichloro-1,2-phenylenediamine

: 882977-67-5
2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

Guidance literature:: Multi-step reaction with 5 steps

1: aq. HCl / 100 °C

2: 52 percent / NaOH; benzyltriethylammonium chloride / acetonitrile

3: 68 percent / Burgess' inner salt / tetrahydrofuran

4: 35 percent / trichloroisocyanuric acid / acetone; H₂O

5: NaOH / methanol

With hydrogenchloride; sodium hydroxide; trichloroisocyanuric acid; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; methanol; water; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2006.10.071

Reference yield:

: 929079-70-9
C₁₀H₁₀N₂Cl₂O

: 882977-67-5
2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / NaOH; benzyltriethylammonium chloride / acetonitrile

2: 68 percent / Burgess' inner salt / tetrahydrofuran

3: 35 percent / trichloroisocyanuric acid / acetone; H₂O

4: NaOH / methanol

With sodium hydroxide; trichloroisocyanuric acid; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; methanol; water; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2006.10.071

Reference yield:

: 882977-74-4
5,6-dichloro-1-methyl-2-isopropenyl-1H-benzimidazole

: 882977-67-5
2-(5,6-dichloro-1-methyl-1H-benzoimidazol-2-yl)-1-phenylmethanesulfanyl-propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / trichloroisocyanuric acid / acetone; H₂O

2: NaOH / methanol

With sodium hydroxide; trichloroisocyanuric acid; In methanol; water; acetone;
DOI:10.1016/j.bmcl.2006.10.071