(S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

Base Information

Chemical Name:(S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one
CAS No.:1417826-98-2
Molecular Formula:C₂₆H₂₆N₂O₅
Molecular Weight:446.503
Hs Code.:

Synonyms:(S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

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Chemical Property of (S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

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Technology Process of (S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

There total 4 articles about (S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 4118-36-9
6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

: C₂₁H₁₉N₂O₆Pol

: C₁₇H₁₈NO₄Pol

: 1417826-98-2
(S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

: (R)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-pent-4-en-1-one

Guidance literature:: In tetrahydrofuran; at 45 ℃; not specified Resolution of racemate; Flow reactor;
DOI:10.1038/nchem.2681

Reference yield: 32.0%

: 1417826-98-2
(S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

: 178032-64-9
(R)-(+)-6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

: 136905-00-5
(S)-(-)-6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: In dichloromethane; for 48h;

Reference yield:

: 4118-36-9
6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

: C₃₀H₂₈N₃O₇Pol

: 1417826-98-2
(S)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

: (R)-1-(6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-nitrophenyl)propan-1-one

: 178032-64-9
(R)-(+)-6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: In dichloromethane; at 23 ℃; for 48h; aminomethyl polystyrene resin Inert atmosphere; Resolution of racemate;
DOI:10.1002/anie.201204991