(2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol

Base Information

Chemical Name:(2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol
CAS No.:595560-05-7
Molecular Formula:C₄₃H₄₅NO₅
Molecular Weight:655.834
Hs Code.:

Synonyms:(2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol

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Chemical Property of (2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol

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Technology Process of (2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol

There total 2 articles about (2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 595560-00-2
(2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-(2-trimethylsilylethynyl)-1,2,3,4,5-hexanepentol

: 595560-05-7
(2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol

Guidance literature:: With sodium hydroxide; In methanol; diethyl ether; water; at 20 ℃; for 1h;
DOI:10.1016/S0040-4020(03)00631-8

Reference yield:

: (2R,3S,4R,5S)-6-N-benzylhydroxylamino-1,3,4,5-O-tetrabenzyl-6-(2-trimethylsilylethynyl)-1,2,3,4,5-hexanepentol

: 595560-05-7
(2R,3S,4R,5S,6S)-6-benzylamino-1,3,4,5-O-tetrabenzyl-6-ethynyl-1,2,3,4,5-hexanepentol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Cu(OCOCH₃)2*H₂O; acetic acid; Zn / H₂O / 1 h / 20 - 70 °C

2: NaOH / diethyl ether; methanol; H₂O / 1 h / 20 °C

With sodium hydroxide; copper diacetate; acetic acid; zinc; In methanol; diethyl ether; water;
DOI:10.1016/S0040-4020(03)00631-8