Technology Process of C32H43N7O5
There total 11 articles about C32H43N7O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C34H47N7O5;
With
water; sodium hydroxide;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 20h;
With
hydrogenchloride;
In
tetrahydrofuran; methanol; water;
pH=7;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diethylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C
2.1: potassium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / tert-butyl alcohol / 80 °C / Inert atmosphere of N2
3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C
4.1: 20 h / 60 °C
5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 h / 20 °C
5.2: pH 7
With
water; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; diethylazodicarboxylate; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; tert-butyl alcohol;
2.1: Buchwald-Hartwig Pd catalyzed aryl C-N formation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / tert-butyl alcohol / 80 °C / Inert atmosphere of N2
2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C
3.1: 20 h / 60 °C
4.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 h / 20 °C
4.2: pH 7
With
water; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; tert-butyl alcohol;
1.1: Buchwald-Hartwig Pd catalyzed aryl C-N formation;
