C₇₅H₁₀₈N₂O₁₆Si₂

Base Information

Chemical Name:C₇₅H₁₀₈N₂O₁₆Si₂
CAS No.:245736-60-1
Molecular Formula:C₇₅H₁₀₈N₂O₁₆Si₂
Molecular Weight:1349.86
Hs Code.:

C<sub>75</sub>H<sub>108</sub>N<sub>2</sub>O<sub>16</sub>Si<sub>2</sub>

Synonyms:C₇₅H₁₀₈N₂O₁₆Si₂

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Chemical Property of C₇₅H₁₀₈N₂O₁₆Si₂

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Technology Process of C₇₅H₁₀₈N₂O₁₆Si₂

There total 41 articles about C₇₅H₁₀₈N₂O₁₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 245736-60-1
C₇₅H₁₀₈N₂O₁₆Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) 2,6-lutidine, 2.) KO-t-Bu / 1.) CH₂Cl₂, -78 deg C, 2.) THF, -10 deg C

2: DIBAL-H / tetrahydrofuran / -78 - 23 °C

3: Br₂, Ph₃P, imidazole, 2-methyl-2-butene / CH₂Cl₂

4: 78 percent / AgNO₂ / diethyl ether

5: 1.) 3-ClPhNCO, i-Pr₂NEt / 1.) PhMe, 2.) PhMe, 90 deg C

6: PPTS / methanol / 0 °C

7: SO₃*pyr, i-Pr₂NEt / dimethylsulfoxide; CH₂Cl₂ / -15 °C

8: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

9: 100 percent / 2,6-lutidine / CH₂Cl₂ / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; silver(I) nitrite; 2-methyl-but-2-ene; pyridine-SO₃ complex; N,N-dimethyl-ethanamine; dicyclohexylboron chloride; potassium tert-butylate; bromine; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; m-chlorophenyl isocyanate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja990789h

Reference yield:

: 100-39-0
benzyl bromide

: 245736-60-1
C₇₅H₁₀₈N₂O₁₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: Cs₂CO₃ / dimethylformamide; CH₂Cl₂

2: aq. OsO₄, NMO / tetrahydrofuran; 2-methyl-propan-2-ol

3: aq. NaIO₄, NaHCO₃ / tetrahydrofuran; 2-methyl-propan-2-ol

4: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

5: 98 percent / 2,6-lutidine / CH₂Cl₂ / -78 °C

6: 1.) 3-ClPhNCO, i-Pr₂NEt / 1.) PhMe, 2.) PhMe, 90 deg C

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; N,N-dimethyl-ethanamine; dicyclohexylboron chloride; sodium hydrogencarbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; m-chlorophenyl isocyanate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja990789h

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 245736-60-1
C₇₅H₁₀₈N₂O₁₆Si₂

Guidance literature:: Multi-step reaction with 19 steps

1: NaH / dimethylformamide; tetrahydrofuran

2: HCl / methanol; diethyl ether / 0 °C

3: (COCl)2, DMSO, i-Pr₂NEt / -78 - -30 °C

4: 73 percent / TiCl₂(O-i-Pr)2 / CH₂Cl₂ / -78 - 0 °C

5: Et₂BOMe, NaBH₄ / tetrahydrofuran; methanol / -78 °C

6: HCl

7: DIBAL-H / CH₂Cl₂ / -78 °C

8: 1.) Bu₂BOTf, i-Pr₂NEt / 1.) CH₂Cl₂, 0 deg C, 2.) CH₂Cl₂, -78 deg C

9: 100 percent / (COCl)2, DMSO, i-Pr₂NEt / -78 - 0 °C

10: 82 percent / TsOH / acetonitrile / -22 °C

11: 100 percent / (COCl)2, DMSO, Et₃N / -78 - 0 °C

12: LDA / 1 h / -78 °C

13: LiOOH / tetrahydrofuran; dimethylformamide; H₂O / 0 - 23 °C

14: Cs₂CO₃ / dimethylformamide; CH₂Cl₂

15: aq. OsO₄, NMO / tetrahydrofuran; 2-methyl-propan-2-ol

16: aq. NaIO₄, NaHCO₃ / tetrahydrofuran; 2-methyl-propan-2-ol

17: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

18: 98 percent / 2,6-lutidine / CH₂Cl₂ / -78 °C

19: 1.) 3-ClPhNCO, i-Pr₂NEt / 1.) PhMe, 2.) PhMe, 90 deg C

With 2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; titanium(IV) dichlorodiisopropylate; oxalyl dichloride; lithium hydroperoxide; N,N-dimethyl-ethanamine; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; dicyclohexylboron chloride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; m-chlorophenyl isocyanate; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja990789h