(2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

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Chemical Name:(2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate
CAS No.:130096-78-5
Molecular Formula:C₂₂H₂₅NO₄S₂
Molecular Weight:431.577
Hs Code.:

Synonyms:(2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

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Chemical Property of (2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

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Technology Process of (2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

There total 7 articles about (2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 130096-78-5
(2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) n-BuLi / 1) THf, hexane, -78 deg C, 30 min, 2) THF, -78 deg C, 30 min

2: Et₃SiH, CF₃COOH / 18 h / Ambient temperature

3: Et₃N / CH₂Cl₂ / 4 h / Ambient temperature

With triethylsilane; n-butyllithium; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo00001a045

Reference yield:

: 676449-09-5
(2R,3R)-3-hydroxy-2-(4-methoxybenzyl)pyrrolidine

: 130096-78-5
(2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 4 h / Ambient temperature

With triethylamine; In dichloromethane;
DOI:10.1021/jo00001a045

Reference yield:

: 123287-88-7
(2S,3R)-tert-butyl 3-((tert-butyldimethylsilyl)oxy)-2-(hydroxymethyl)pyrrolidine-1-carboxylate

: 130096-78-5
(2R,3R)-1-(Benzyloxycarbonyl)-2-<(3-methoxyphenyl)-methyl>pyrrolidin-3-yl S-Methyl Xanthate

Guidance literature:: Multi-step reaction with 5 steps

1: 1) (CF₃CO)2O, DMSO, 2) Et₃N / 1) CH₂Cl₂, -78 deg C, 2h, 2) to 0 deg C, 1h

2: 1) n-BuLi / 1) THf, hexane, -78 deg C, 30 min, 2) THF, -78 deg C, 30 min

3: Et₃SiH, CF₃COOH / 18 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 4 h / Ambient temperature

With triethylsilane; n-butyllithium; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1021/jo00001a045