3-(But-3-en-1-yl)benzaldehyde

Base Information

Chemical Name:3-(But-3-en-1-yl)benzaldehyde
CAS No.:358751-00-5
Molecular Formula:C11H12 O
Molecular Weight:160.216
Hs Code.:2912299000
European Community (EC) Number:837-454-1
DSSTox Substance ID:DTXSID40448321
Wikidata:Q82267294
Mol file:358751-00-5.mol

Synonyms:3-(But-3-en-1-yl)benzaldehyde;358751-00-5;3-but-3-enylbenzaldehyde;3-(3-Buten-1-yl)benzaldehyde;SCHEMBL17006079;DTXSID40448321;SPSGCPQLOUNVMU-UHFFFAOYSA-N;AT32510;EN300-7355071;Z1511874801

Suppliers and Price of 3-(But-3-en-1-yl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
3-(But-3-en-1-yl)benzaldehyde
1g
$ 1204.00

Total 1 raw suppliers

Chemical Property of 3-(But-3-en-1-yl)benzaldehyde

Chemical Property:

PSA：17.07000
LogP:2.61770
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:160.088815002
Heavy Atom Count:12
Complexity:151

Purity/Quality:: 3-(But-3-en-1-yl)benzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCC1=CC(=CC=C1)C=O

Technology Process of 3-(But-3-en-1-yl)benzaldehyde

There total 4 articles about 3-(But-3-en-1-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 161173-98-4
1-bromo-3-(but-3-en-1-yl)benzene

: 358751-00-5
3-(but-3-en-1-yl)benzaldehyde

Guidance literature:: 1-bromo-3-(but-3-en-1-yl)benzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

N,N-dimethyl-formamide; In tetrahydrofuran; at -78 - 20 ℃; for 3.5h;

Reference yield:

: 1-but-3-enyl-3-dimethoxymethyl-benzene

: 358751-00-5
3-(but-3-en-1-yl)benzaldehyde

Guidance literature:: With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 4h;
DOI:10.1081/SCC-100103323

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 358751-00-5
3-(but-3-en-1-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 3 h / 20 °C / Reflux

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

2.2: 3.5 h / -78 - 20 °C

With n-butyllithium; In tetrahydrofuran;