C₅₆H₄₈O₁₃

Base Information

• Chemical Name: C₅₆H₄₈O₁₃
• CAS No.: 1309453-94-8
• Molecular Formula: C₅₆H₄₈O₁₃
• Molecular Weight: 928.989
• Mol file: 1309453-94-8.mol

Synonyms:C₅₆H₄₈O₁₃

Chemical Property of C₅₆H₄₈O₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₆H₄₈O₁₃

There total 8 articles about C₅₆H₄₈O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C62H54O16 (1309453-97-1) → C56H48O13 (1309453-94-8)

Guidance literature:

With acetyl chloride; In methanol; dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.tetlet.2011.04.040

Reference yield:

7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-3,5-dihydroxy-4H-chromen-4-one (183067-65-4) → C56H48O13 (1309453-94-8)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; potassium carbonate / chloroform; water / 12 h / 50 °C

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

3: acetyl chloride / methanol; dichloromethane / 24 h / 20 °C

With tetrabutylammomium bromide; potassium carbonate; acetyl chloride; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2011.04.040

Reference yield:

1,2,4,6-tetra-O-acetyl-3-O-benzoyl-β-D-glucopyranose (28219-87-6) → C56H48O13 (1309453-94-8)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogen bromide / dichloromethane; acetic acid / 0 - 20 °C

2: tetrabutylammomium bromide; potassium carbonate / chloroform; water / 12 h / 50 °C

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

4: acetyl chloride / methanol; dichloromethane / 24 h / 20 °C

With tetrabutylammomium bromide; hydrogen bromide; potassium carbonate; acetyl chloride; In methanol; dichloromethane; chloroform; water; acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2011.04.040

upstream raw materials:

7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-3,5-dihydroxy-4H-chromen-4-one

C₅₅H₄₈O₁₆

C₆₂H₅₄O₁₆

1,2,4,6-tetra-O-acetyl-3-O-benzoyl-β-D-glucopyranose

Downstream raw materials:

C₈₃H₇₀O₂₀

Refernces