N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

Base Information

Chemical Name:N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide
CAS No.:264887-69-6
Molecular Formula:C₂₁H₃₃N₃O₄
Molecular Weight:391.511
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

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Chemical Property of N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

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Technology Process of N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

There total 4 articles about N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 36360-62-0
N-benzyloxycarbonyl-L-norleucine succinimide ester

: 264887-68-5
L-norleucine methylamide

: 264887-69-6
N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

Guidance literature:: With triethylamine; In 1,2-dimethoxyethane; water; at 20 ℃;
DOI:10.1021/jm990226g

Reference yield:

: C₁₉H₂₇NO₅

: 264887-69-6
N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 20 °C

2: 99 percent / H₂; glacial acetic acid / Pd/C / methanol / 3 h / 25 °C / 1551.49 Torr

3: 51 percent / Et₃N / H₂O; 1,2-dimethoxy-ethane / 20 °C

With hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; 1: Condensation / 2: Hydrogenation / 3: Condensation;
DOI:10.1021/jm990226g

Reference yield:

: 264887-67-4
N-benzyloxycarbonyl-L-norleucine methylamide

: 264887-69-6
N-benzyloxycarbonyl-L-norleucyl-L-norleucine methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / H₂; glacial acetic acid / Pd/C / methanol / 3 h / 25 °C / 1551.49 Torr

2: 51 percent / Et₃N / H₂O; 1,2-dimethoxy-ethane / 20 °C

With hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In methanol; 1,2-dimethoxyethane; water; 1: Hydrogenation / 2: Condensation;
DOI:10.1021/jm990226g