methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

Base Information

Chemical Name:methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate
CAS No.:176502-43-5
Molecular Formula:C₁₆H₁₈O₃
Molecular Weight:258.317
Hs Code.:

Synonyms:methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

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Technology Process of methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

There total 5 articles about methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 591-50-4
iodobenzene

: 131190-10-8
methyl 2-acetyl-6-heptynoate

: 176502-43-5
methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

Guidance literature:: With copper(l) iodide; tributyl-amine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; for 6h;
DOI:10.1021/jo9600619

Reference yield: 58.0%

: 34886-50-5
(5-iodopent-1-yn-1-yl)benzene

: 105-45-3
acetoacetic acid methyl ester

: 176502-43-5
methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

Guidance literature:: acetoacetic acid methyl ester; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

(5-iodopent-1-yn-1-yl)benzene; In tetrahydrofuran; N,N-dimethyl-formamide; for 15h; Inert atmosphere;
DOI:10.1021/ol802079r

Reference yield:

: 57718-13-5
(5-bromo-pent-1-ynyl)-benzene

: 105-45-3
acetoacetic acid methyl ester

: 176502-43-5
methyl 2-(1-oxoethyl)-7-phenyl-6-heptynoate

Guidance literature:: acetoacetic acid methyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

(5-bromo-pent-1-ynyl)-benzene; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at 66 ℃; Inert atmosphere;
DOI:10.1021/ol200471w