(3S,4R)-3-<amino>-4-methyl-2-oxetanone

Base Information

Chemical Name:(3S,4R)-3-<amino>-4-methyl-2-oxetanone
CAS No.:131131-08-3
Molecular Formula:C₁₈H₂₄N₂O₅
Molecular Weight:348.399
Hs Code.:

(3S,4R)-3-<<N-(tert-butoxycarbonyl)-D-phenylalaninyl>amino>-4-methyl-2-oxetanone

Synonyms:(3S,4R)-3-<amino>-4-methyl-2-oxetanone

Suppliers and Price of (3S,4R)-3-<amino>-4-methyl-2-oxetanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (3S,4R)-3-<amino>-4-methyl-2-oxetanone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3S,4R)-3-<amino>-4-methyl-2-oxetanone

There total 2 articles about (3S,4R)-3-<amino>-4-methyl-2-oxetanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 131131-08-3
(3S,4R)-3-<amino>-4-methyl-2-oxetanone

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at -5 ℃; for 0.333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; for 0.5h; Inert atmosphere;

Reference yield:

: 18942-49-9
Boc-D-Phe-OH

: 131131-06-1
(3S,4R)-2-methyl-4-oxo-3-oxetanylammonium toluene-4-sulfonate

: 131131-08-3
(3S,4R)-3-<amino>-4-methyl-2-oxetanone

Guidance literature:: With pyridine; chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1) CH₂Cl₂, -5 deg C, 20 min., 2) a) -5 deg C, 30 min., b) 20 deg C, overnight;
DOI:10.1021/jo00003a062