ethyl 2-butoxybenzoate

Base Information

• Chemical Name: ethyl 2-butoxybenzoate
• CAS No.: 289894-50-4
• Molecular Formula: C₁₃H₁₈O₃
• Molecular Weight: 222.284

Synonyms:ethyl 2-butoxybenzoate

Chemical Property of ethyl 2-butoxybenzoate

Chemical Property:

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Technology Process of ethyl 2-butoxybenzoate

There total 1 articles about ethyl 2-butoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

1-bromo-butane (109-65-9) + 2-hydroxy-benzoic acid ethyl ester (118-61-6) → ethyl 2-butoxybenzoate (289894-50-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 3h;

DOI:10.1021/ja031632z

Reference yield: 89.0%

ethyl 2-butoxybenzoate (289894-50-4) → 2-butoxybenzoic acid (2200-81-9)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; for 1h; Heating;

DOI:10.1021/ja031632z

Reference yield: 47.0%

ethyl 2-butoxybenzoate (289894-50-4) + 9-amino-9-deoxyepicinchonine → 2-butoxy-N-(9-deoxyepicinchonin-9-yl)benzamide

Guidance literature:

With trimethylaluminum; In toluene; at 20 ℃; for 0.25h;

DOI:10.1002/1099-0690(200006)2000:11<2119::aid-ejoc2119>3.0.co;2-5

upstream raw materials:

1-bromo-butane

2-hydroxy-benzoic acid ethyl ester

Downstream raw materials:

2-butoxybenzoic acid

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