1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide

Base Information

Chemical Name:1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide
CAS No.:1227203-11-3
Molecular Formula:Br*C₂₈H₃₃N₂
Molecular Weight:477.487
Hs Code.:

Synonyms:1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide

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Chemical Property of 1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide

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Technology Process of 1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide

There total 1 articles about 1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 180127-82-6
1-(4-(tert-butyl)benzyl)-1H-benzo[d]imidazole

: 4761-00-6
2,4,6-trimethylbenzylbromide

: 1227203-11-3
1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2013.01.025

Reference yield: 85.0%

: 1227203-11-3
1-(2,4,6-trimethylbenzyl)-3-(4-tert-butylbenzyl)benzimidazolium bromide

: 20667-12-3
silver(l) oxide

: bromo[1-(2,4,6-trimethylbenzyl)-3-(4-tert-butyl)benzimidazolylidene]silver(I)

Guidance literature:: With molecular sieves; In dichloromethane; (Ar), soln. of benzimidazolium salt, Ag2O (2:1) and activated molecular sieves in CH2Cl2 stirred at room temp for 8 h in the dark; filtered (celite), evapd.(vac.), recrystd.(CH2Cl2/n-hexane) at room temp., elem. anal.;
DOI:10.1016/j.ica.2010.07.034