2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

Base Information

Chemical Name:2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine
CAS No.:194039-64-0
Molecular Formula:C₂₅H₂₉N₇O₃
Molecular Weight:475.55
Hs Code.:

Synonyms:2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

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Chemical Property of 2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

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Technology Process of 2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

There total 4 articles about 2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 113494-35-2
2,4-diamino-5-(4'-fluoro-3'-nitrophenyl)-6-ethylpyrimidine

: 194039-67-3
2-{4-[(N-methylamino)methyl]phenyl}-4,4-dimethyloxazoline

: 194039-64-0
2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

Guidance literature:: With triethylamine; In various solvent(s); at 100 ℃; for 10h;
DOI:10.1021/jm970055k

Reference yield:

: 876-08-4
p-(chloromethyl)benzoyl chloride

: 194039-64-0
2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 12 h / Ambient temperature

2: 75 percent / ethanol / Ambient temperature

3: 83 percent / Et₃N / various solvent(s) / 10 h / 100 °C

With triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm970055k

Reference yield:

: 1642-81-5
p-(chloromethyl)benzoic acid

: 194039-64-0
2,4-diamino-5-(4'-{N-[4''-(4,4-dimethyloxazolin-2-yl)benzyl]amino}-3'-nitrophenyl)-6-ethylpyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂, DMF / tetrahydrofuran / 48 h / Ambient temperature

2: CH₂Cl₂ / 12 h / Ambient temperature

3: 75 percent / ethanol / Ambient temperature

4: 83 percent / Et₃N / various solvent(s) / 10 h / 100 °C

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm970055k