methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate

Base Information

• Chemical Name: methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate
• CAS No.: 1140920-99-5
• Molecular Formula: C₁₃H₁₀ClNO₃S₂
• Molecular Weight: 327.812
• Mol file: 1140920-99-5.mol

Synonyms:methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate

Chemical Property of methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate

There total 3 articles about methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

carbon disulfide (75-15-0,12122-00-8) + dimethyl acetylenedicarboxylate (762-42-5) + 2-CHLOROBENZYLAMINE (89-97-4) → methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate (1140920-99-5)

Guidance literature:

With k-carrageenan/Fe₃O₄ nanocomposite; In water; at 20 ℃; for 0.25h; Green chemistry;

DOI:10.1016/j.catcom.2015.05.002

Reference yield:

C8H8ClNS2 + dimethyl acetylenedicarboxylate (762-42-5) → methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate (1140920-99-5)

Guidance literature:

With β‐cyclodextrin; In water; at 20 ℃; for 0.25h; Green chemistry;

DOI:10.1080/10610278.2014.890200

Reference yield:

2-CHLOROBENZYLAMINE (89-97-4) → methyl 2-[3-((2-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolidin-5-yliden]ethanoate (1140920-99-5)

Guidance literature:

Multi-step reaction with 2 steps

1: β‐cyclodextrin / water / 0.01 h / 20 °C / Green chemistry

2: β‐cyclodextrin / water / 0.25 h / 20 °C / Green chemistry

With β‐cyclodextrin; In water;

DOI:10.1080/10610278.2014.890200

upstream raw materials:

carbon disulfide

dimethyl acetylenedicarboxylate

2-CHLOROBENZYLAMINE