p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside
CAS No.:78499-24-8
Molecular Formula:C₄₉H₅₂N₂O₁₃
Molecular Weight:876.957
Hs Code.:

Synonyms:p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Chemical Property of p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Technology Process of p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

There total 1 articles about p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40615-62-1
p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-β-D-glucopyranoside

: 33639-77-9
perbenzyl fucosyl bromide

: 78499-24-8
p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: tetraethylammonium bromide; Multistep reaction; 1.) dichloromethane, 2 h, r.t; 2.) dichloromethane, HCONMe₂, 5 d, r.t.;
DOI:10.1016/S0008-6215(00)86027-9

Reference yield: 74.0%

: 78499-24-8
p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

: 78489-58-4
p-nitrophenyl 2-acetamido-2-deoxy-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With acetic acid; at 100 ℃; for 0.333333h;
DOI:10.1016/S0008-6215(00)86027-9

Reference yield:

: 78499-24-8
p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

: 78489-59-5
hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / 70percent acetic acid / 0.33 h / 100 °C

2: 72 percent / 0.05M HCl / 10percent Pd-C / methanol / 48 h

With hydrogenchloride; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1016/S0008-6215(00)86027-9