hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

Base Information

Chemical Name:hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside
CAS No.:78489-59-5
Molecular Formula:C₂₀H₃₀N₂O₁₀*ClH
Molecular Weight:494.927
Hs Code.:

Synonyms:hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

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Chemical Property of hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

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Technology Process of hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

There total 4 articles about hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 78489-58-4
p-nitrophenyl 2-acetamido-2-deoxy-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

: 78489-59-5
hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; palladium on activated charcoal; In methanol; for 48h;
DOI:10.1016/S0008-6215(00)86027-9

Reference yield:

: 40615-62-1
p-nitrophenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-β-D-glucopyranoside

: 78489-59-5
hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) tetraethylammonium bromide / 1.) dichloromethane, 2 h, r.t; 2.) dichloromethane, HCONMe₂, 5 d, r.t.

2: 74 percent / 70percent acetic acid / 0.33 h / 100 °C

3: 72 percent / 0.05M HCl / 10percent Pd-C / methanol / 48 h

With hydrogenchloride; acetic acid; palladium on activated charcoal; tetraethylammonium bromide; In methanol;
DOI:10.1016/S0008-6215(00)86027-9

Reference yield:

: 33639-77-9
perbenzyl fucosyl bromide

: 78489-59-5
hydrochloride of p-aminophenyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) tetraethylammonium bromide / 1.) dichloromethane, 2 h, r.t; 2.) dichloromethane, HCONMe₂, 5 d, r.t.

2: 74 percent / 70percent acetic acid / 0.33 h / 100 °C

3: 72 percent / 0.05M HCl / 10percent Pd-C / methanol / 48 h

With hydrogenchloride; acetic acid; palladium on activated charcoal; tetraethylammonium bromide; In methanol;
DOI:10.1016/S0008-6215(00)86027-9