C₃₂H₃₈N₂O₅

Base Information

• Chemical Name: C₃₂H₃₈N₂O₅
• CAS No.: 1158857-84-1
• Molecular Formula: C₃₂H₃₈N₂O₅
• Molecular Weight: 530.664
• Mol file: 1158857-84-1.mol

Synonyms:C₃₂H₃₈N₂O₅

Chemical Property of C₃₂H₃₈N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₂H₃₈N₂O₅

There total 2 articles about C₃₂H₃₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

pyrrolidine (123-75-1) + C29H30Cl3NO5 (1158857-78-3) → C32H38N2O5 (1158857-84-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 25 ℃; Inert atmosphere;

DOI:10.1021/ol900670a

Reference yield:

O-(2,3,4-Tri-O-benzyl-6-deoxy-α-D-glucopyranosyl) trichloroacetimidate (120449-25-4) → C32H38N2O5 (1158857-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; silver trifluoromethanesulfonate / dichloromethane / 0.5 h / 25 °C / Schlenk technique; Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 25 °C / Schlenk technique; Inert atmosphere

With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; silver trifluoromethanesulfonate; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/chem.201402433

upstream raw materials:

pyrrolidine

C₂₉H₃₀Cl₃NO₅

O-(2,3,4-Tri-O-benzyl-6-deoxy-α-D-glucopyranosyl) trichloroacetimidate