C₃₆H₃₀Cl₂O₁₂

Base Information

Chemical Name:C₃₆H₃₀Cl₂O₁₂
CAS No.:244262-88-2
Molecular Formula:C₃₆H₃₀Cl₂O₁₂
Molecular Weight:725.533
Hs Code.:

C<sub>36</sub>H<sub>30</sub>Cl<sub>2</sub>O<sub>12</sub>

Synonyms:C₃₆H₃₀Cl₂O₁₂

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Chemical Property of C₃₆H₃₀Cl₂O₁₂

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Technology Process of C₃₆H₃₀Cl₂O₁₂

There total 9 articles about C₃₆H₃₀Cl₂O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 244262-61-1
1,1-bis[3,3-(3'-chloro-4'-methoxy-5'-methoxycarbonylbenzyl)-4-methoxy-5-methoxycarbonylphenyl]-2-chloroethane

: 244262-88-2
C₃₆H₃₀Cl₂O₁₂

Guidance literature:: With potassium hydroxide; In methanol; for 12h; Heating;
DOI:10.1021/jo990177f

Reference yield:

: 89-55-4
5-bromosalicyclic acid

: 244262-88-2
C₃₆H₃₀Cl₂O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1: 72 percent / TFA / 16 h / 90 °C / Acid hydrolysis

2: 90 percent / NaOH; NaBH₄ / ethanol; H₂O / 4 h / 0 °C

3: conc. H₂SO₄ / methanol / 12 h / 0 - 20 °C

4: 32 percent / H₂SO₄ / Heating

5: 77 percent / NaOH; Zn dust / Acid hydrolysis

6: 65 percent / H₂SO₄ / 36 h / 80 °C

7: 30 percent / H₂SO₄; AcOH / 0 - 20 °C

8: 56.8 percent / K₂CO₃ / dimethylformamide / 20 °C

9: 90 percent / KOH / methanol / 12 h / Heating

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; sulfuric acid; potassium carbonate; acetic acid; trifluoroacetic acid; zinc; In methanol; ethanol; water; N,N-dimethyl-formamide; 1: Formylation / 2: Reduction / 3: Substitution / 4: Esterification / 5: Reduction / 6: Esterification / 7: Substitution / 8: Methylation / 9: Elimination;
DOI:10.1021/jo990177f

Reference yield:

: 134948-41-7
5-bromo-3-formyl-2-hydroxybenzoic acid

: 244262-88-2
C₃₆H₃₀Cl₂O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / NaOH; NaBH₄ / ethanol; H₂O / 4 h / 0 °C

2: conc. H₂SO₄ / methanol / 12 h / 0 - 20 °C

3: 32 percent / H₂SO₄ / Heating

4: 77 percent / NaOH; Zn dust / Acid hydrolysis

5: 65 percent / H₂SO₄ / 36 h / 80 °C

6: 30 percent / H₂SO₄; AcOH / 0 - 20 °C

7: 56.8 percent / K₂CO₃ / dimethylformamide / 20 °C

8: 90 percent / KOH / methanol / 12 h / Heating

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; sulfuric acid; potassium carbonate; acetic acid; zinc; In methanol; ethanol; water; N,N-dimethyl-formamide; 1: Reduction / 2: Substitution / 3: Esterification / 4: Reduction / 5: Esterification / 6: Substitution / 7: Methylation / 8: Elimination;
DOI:10.1021/jo990177f