(+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Base Information

Chemical Name:(+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid
CAS No.:1642790-75-7
Molecular Formula:C₁₀H₁₃N₂O₅P
Molecular Weight:272.197
Hs Code.:

Synonyms:(+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Suppliers and Price of (+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

There total 3 articles about (+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1642790-73-5
(+/-)-diethyl ((1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)-methyl)phosphonate

: 1642790-75-7
(+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Guidance literature:: (+/-)-diethyl ((1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)-methyl)phosphonate; With trimethylsilyl bromide; In methanol; at 20 ℃; Schlenk technique; Inert atmosphere;

With hydrogenchloride; In water; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4ra00757c

Reference yield:

: 1639810-06-2
(E)-diethyl (3-(1-(benzyloxy)-3-phenylureido)prop-1-en-1-yl)phosphonate

: 1642790-75-7
(+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 48 h / 70 °C / Inert atmosphere

2.1: 10% palladium hydroxide on charcoal; hydrogen / ethanol / 3 h / 20 °C / Schlenk technique; Inert atmosphere

3.1: trimethylsilyl bromide / methanol / 20 °C / Schlenk technique; Inert atmosphere

3.2: Schlenk technique; Inert atmosphere

With trimethylsilyl bromide; 10% palladium hydroxide on charcoal; potassium tert-butylate; hydrogen; In tetrahydrofuran; methanol; ethanol;
DOI:10.1039/c4ra00757c

Reference yield:

: 1642790-70-2
(+/-)-diethyl ((1-(benzyloxy)-3-phenyl-2-oxoimidazolidin-4-yl)-methyl)phosphonate

: 1642790-75-7
(+/-)-(1-hydroxy-3-phenyl-2-oxoimidazolidin-4-yl)methylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 10% palladium hydroxide on charcoal; hydrogen / ethanol / 3 h / 20 °C / Schlenk technique; Inert atmosphere

2.1: trimethylsilyl bromide / methanol / 20 °C / Schlenk technique; Inert atmosphere

2.2: Schlenk technique; Inert atmosphere

With trimethylsilyl bromide; 10% palladium hydroxide on charcoal; hydrogen; In methanol; ethanol;
DOI:10.1039/c4ra00757c