6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate
CAS No.:958248-97-0
Molecular Formula:C₃₀H₃₂Cl₆N₂O₁₀
Molecular Weight:793.309
Hs Code.:

6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

Synonyms:6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

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Chemical Property of 6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

Chemical Property:

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Technology Process of 6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

There total 4 articles about 6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952429-82-2
[(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-6-hydroxymethyl-4-(4-methoxy-benzyloxy)-tetrahydro-pyran-3-yl]-carbamic acid 2,2,2-trichloro-ethyl ester

: 958248-97-0
6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / [Ir(cod)(H)(MePh₂P)2]PF₆ / tetrahydrofuran / 3 h / 20 °C

2: 98 percent / molecular sieves 4 Angstroem; 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h / 0 - 20 °C

3: 85 percent / I₂ / tetrahydrofuran; H₂O / 2 h / 20 °C

4: Cs₂CO₃ / CH₂Cl₂ / 1 h / 20 °C

With dmap; 4 A molecular sieve; iodine; caesium carbonate; [Ir(cod)(H)(MePh₂P)2]PF₆; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2007.07.036

Reference yield:

: 6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 958248-97-0
6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With caesium carbonate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2007.07.036

Reference yield:

: 952429-83-3
C₂₇H₃₂Cl₃NO₈

: 958248-97-0
6-O-allyloxycarbonyl-4-O-benzyl-2-deoxy-3-O-(4-methoxybenzyl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / molecular sieves 4 Angstroem; 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h / 0 - 20 °C

2: 85 percent / I₂ / tetrahydrofuran; H₂O / 2 h / 20 °C

3: Cs₂CO₃ / CH₂Cl₂ / 1 h / 20 °C

With dmap; 4 A molecular sieve; iodine; caesium carbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2007.07.036