C₃₁H₂₈O₆

Base Information

Chemical Name:C₃₁H₂₈O₆
CAS No.:1262422-34-3
Molecular Formula:C₃₁H₂₈O₆
Molecular Weight:496.56
Hs Code.:

C<sub>31</sub>H<sub>28</sub>O<sub>6</sub>

Synonyms:C₃₁H₂₈O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₂₈O₆

Chemical Property:

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Technology Process of C₃₁H₂₈O₆

There total 16 articles about C₃₁H₂₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1262422-33-2
C₃₁H₃₀O₆

: 1262422-34-3
C₃₁H₂₈O₆

Guidance literature:: With PCC on Al₂O₃; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/ejoc.201001023

Reference yield:

: 1186304-20-0
{4-[5-([1,3]-dioxan-2-yl)-2-methoxyphenoxy]benzyl}triphenylphosphonium bromide

: 1262422-34-3
C₃₁H₂₈O₆

Guidance literature:: Multi-step reaction with 4 steps

1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux

2: 5% Pd(II)/C(eggshell); hydrogen; triethylamine / ethyl acetate / 24 h / 20 °C / 2250.23 Torr / Autoclave

3: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C

4: PCC on Al₂O₃ / dichloromethane / 16 h / 20 °C

With hydrogenchloride; 18-crown-6 ether; 5% Pd(II)/C(eggshell); hydrogen; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; 1: Wittig reaction;
DOI:10.1002/ejoc.201001023

Reference yield:

: 621-59-0
isovanillin

: 1262422-34-3
C₃₁H₂₈O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetra-N-butylammonium tribromide; orthoformic acid triethyl ester / 6 h / 65 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 165 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C

4.1: acetonitrile / 6 h / Reflux

4.2: 12 h / Reflux

5.1: 18-crown-6 ether; potassium carbonate / dichloromethane / 24 h / Reflux

6.1: 5% Pd(II)/C(eggshell); hydrogen; triethylamine / ethyl acetate / 24 h / 20 °C / 2250.23 Torr / Autoclave

7.1: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C

8.1: PCC on Al₂O₃ / dichloromethane / 16 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; 18-crown-6 ether; 5% Pd(II)/C(eggshell); hydrogen; tetra-N-butylammonium tribromide; potassium carbonate; triethylamine; orthoformic acid triethyl ester; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 5.1: Wittig reaction;
DOI:10.1002/ejoc.201001023