2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester

Base Information

• Chemical Name: 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester
• CAS No.: 286372-23-4
• Molecular Formula: C₁₂H₁₂N₂O₉S
• Molecular Weight: 360.301

Synonyms:2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester

Chemical Property of 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester

Chemical Property:

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Technology Process of 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester

There total 3 articles about 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Methyl thioglycolate (2365-48-2) + 2-fluoro-6-methoxy-3,5-dinitro-benzoic acid methyl ester (251089-58-4) → 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester (286372-23-4)

Guidance literature:

Methyl thioglycolate; With lithium hydroxide; In N,N-dimethyl-formamide; for 3h;

2-fluoro-6-methoxy-3,5-dinitro-benzoic acid methyl ester; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Further stages.;

DOI:10.1021/jo991958j

Reference yield:

methyl 2-fluoro-6-methoxybenzoate (178747-79-0) → 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester (286372-23-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / NO₂BF₄

With nitronium tetrafluoborate;

DOI:10.1021/ol991049g

Reference yield:

LiSCH2CO2Me + 2-fluoro-6-methoxy-3,5-dinitro-benzoic acid methyl ester (251089-58-4) → 2-methoxy-6-methoxycarbonylmethylsulfanyl-3,5-dinitro-benzoic acid methyl ester (286372-23-4)

Guidance literature:

DOI:10.1021/ol991049g

upstream raw materials:

Methyl thioglycolate

2-fluoro-6-methoxy-3,5-dinitro-benzoic acid methyl ester

methyl 2-fluoro-6-methoxybenzoate

Downstream raw materials:

8-(1-benzenesulfonyl-4-{6-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-pent-3-enyl)-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

8-(1-benzenesulfonyl-4-{6-[10-(tert-butyl-dimethyl-silanyloxy)-8-methoxy-deca-2,4,6-trienyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-pent-3-enyl)-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

toluene-4-sulfonic acid 6-benzyloxycarbonylamino-7-methoxy-3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-8-ylmethyl ester

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