2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

Base Information

Chemical Name:2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid
CAS No.:959861-52-0
Molecular Formula:C₁₃H₁₈O₂₀S₄
Molecular Weight:622.538
Hs Code.:

Synonyms:2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

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Chemical Property of 2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

Chemical Property:

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Technology Process of 2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

There total 5 articles about 2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 959861-61-1
5-((R)-2,3-dihydroxypropoxy)-2-((S)-2,3-dihydroxypropoxy)benzoic acid

: 959861-52-0
2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

Guidance literature:: With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 40 ℃; for 16h;

Reference yield:

: 79250-48-9
methyl 2,5-bis(allyloxy)benzoate

: 959861-52-0
2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: methanesulfonamide; AD-mix-α / tert-butyl alcohol; water / 12 h / 0 °C

2: potassium hydroxide; water / ethanol / 6 h / 60 °C

3: AD-mix β; methyl (S)-5-(2,3-bis(sulfooxy)propoxy)-2-(4-(sulfooxy)butoxy)benzoate / tert-butyl alcohol; water / 12 h / 0 °C

4: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 16 h / 40 °C

With methanesulfonamide; AD-mix β; AD-mix-α; methyl (S)-5-(2,3-bis(sulfooxy)propoxy)-2-(4-(sulfooxy)butoxy)benzoate; water; sulfur trioxide trimethylamine complex; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 959861-59-7
methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate

: 959861-52-0
2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; water / ethanol / 6 h / 60 °C

2: AD-mix β; methyl (S)-5-(2,3-bis(sulfooxy)propoxy)-2-(4-(sulfooxy)butoxy)benzoate / tert-butyl alcohol; water / 12 h / 0 °C

3: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 16 h / 40 °C

With AD-mix β; methyl (S)-5-(2,3-bis(sulfooxy)propoxy)-2-(4-(sulfooxy)butoxy)benzoate; water; sulfur trioxide trimethylamine complex; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol;