1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

Base Information

• Chemical Name: 1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol
• CAS No.: 261913-82-0
• Molecular Formula: C₁₉H₁₄F₃I₄NO₃
• Molecular Weight: 868.938

Synonyms:1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

Chemical Property of 1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

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Technology Process of 1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

There total 2 articles about 1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-79-5) → 1-(3,5-diiodo-4-methoxybenzyl)-7-iodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol + 1-(3,5-diiodo-4-methoxybenzyl)-5-iodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-80-8) + 1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-82-0)

Guidance literature:

With N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate; In methanol; dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/jm990463j

Reference yield:

1-(3,5-diiodo-4-methoxybenzyl)-1,2,3,4-tetrahydroisoquinolin-6-ol hydrochloride → 1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-82-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / Et₃N / tetrahydrofuran / 20 °C

2: 12 percent / BTMACl₂I; CaCO₃ / CH₂Cl₂; methanol / 5 h / 20 °C

With N,N,N-trimethylbenzenemethanaminium dichloroiodate; triethylamine; calcium carbonate; In tetrahydrofuran; methanol; dichloromethane; 1: Acylation / 2: Iodination;

DOI:10.1021/jm990463j

Reference yield:

1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-82-0) → 1-(3,5-diiodo-4-methoxy-benzyl)-5,7-diiodo-1,2,3,4-tetrahydro-isoquinolin-6-ol

Guidance literature:

With potassium carbonate; In methanol; for 1h; Heating;

DOI:10.1021/jm990463j

upstream raw materials:

1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

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