1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

Base Information

• Chemical Name: 1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol
• CAS No.: 261913-79-5
• Molecular Formula: C₁₉H₁₆F₃I₂NO₃
• Molecular Weight: 617.145

Synonyms:1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

Chemical Property of 1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

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Technology Process of 1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

There total 1 articles about 1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

trifluoroacetic anhydride (407-25-0) + 1-(3,5-diiodo-4-methoxybenzyl)-1,2,3,4-tetrahydroisoquinolin-6-ol hydrochloride → 1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-79-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jm990463j

Reference yield: 86.0%

1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-79-5) → 1-(3,5-diiodo-4-methoxybenzyl)-5,7-dibromo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-84-2)

Guidance literature:

With bromine; In acetic acid; at 20 ℃; for 4h;

DOI:10.1021/jm990463j

Reference yield: 76.0%

1-(3,5-diiodo-4-methoxybenzyl)-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-79-5) → 1-(3,5-diiodo-4-methoxybenzyl)-5-bromo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol + 1-(3,5-diiodo-4-methoxybenzyl)-5,7-dibromo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol (261913-84-2)

Guidance literature:

With pyridinium hydrobromide perbromide; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1021/jm990463j

upstream raw materials:

trifluoroacetic anhydride

Downstream raw materials:

1-(3,5-diiodo-4-methoxybenzyl)-5,7-dibromo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

1-(3,5-diiodo-4-methoxybenzyl)-5-iodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

1-(3,5-diiodo-4-methoxybenzyl)-5,7-diiodo-2-trifluoroacetyl-1,2,3,4-tetrahydroisoquinolin-6-ol

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