(E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

Base Information

Chemical Name:(E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole
CAS No.:180282-21-7
Molecular Formula:C₁₈H₁₈N₂O₂
Molecular Weight:294.353
Hs Code.:

Synonyms:(E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

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Technology Process of (E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

There total 3 articles about (E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 180282-20-6
(E,E)-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

: 74-88-4
methyl iodide

: 180282-21-7
(E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

Guidance literature:: With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; for 0.5h;
DOI:10.1055/s-1996-4306

Reference yield:

: 4995-09-9
1-nitro-6-phenylhexa-1,3,5-triene

: 180282-21-7
(E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuOK / 1.) THF, -80 deg C, 10 min, 2.) THF, from -80 deg C to -40 deg C, 1 h

2: 99 percent / 50percent aq. KOH, benzyltriethylammonium chloride / CH₂Cl₂ / 0.5 h

With potassium hydroxide; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane;
DOI:10.1055/s-1996-4306

Reference yield:

: 71333-63-6
1-Isocyano-2-methyl-1-tosyl-1-propen

: 180282-21-7
(E,E)-1-methyl-4-nitro-3-(4-phenylbuta-1,3-dienyl)-2-(1-methylethenyl)pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuOK / 1.) THF, -80 deg C, 10 min, 2.) THF, from -80 deg C to -40 deg C, 1 h

2: 99 percent / 50percent aq. KOH, benzyltriethylammonium chloride / CH₂Cl₂ / 0.5 h

With potassium hydroxide; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane;
DOI:10.1055/s-1996-4306