<(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

Base Information

Chemical Name:<(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate
CAS No.:194783-33-0
Molecular Formula:C₂₈H₄₀O₆S
Molecular Weight:504.688
Hs Code.:

Synonyms:<(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

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Technology Process of <(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

There total 7 articles about <(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 194783-32-9
<(2S,3S)-2-(benzyloxy)-8-hydroxynon-3-yl>-p-toluenesulfonate

: 194783-33-0
<(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jm00048a020

Reference yield: 99.0%

: 194783-33-0
<(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

Guidance literature:

Reference yield:

: 34164-50-6
4-penten-1-ylmagnesium bromide

: 194783-33-0
<(2S,3S)-2-(benzyloxy)-8-<(2-tetrahydropyranyl)oxy>non-3-yl>-p-toluenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / Li₂CuCl₄ / diethyl ether / 1 h / -78 °C

2: 97 percent / pyridine / 12 h / Ambient temperature

3: 99 percent / 85percent m-chloroperbenzoic acid / CH₂Cl₂ / Ambient temperature

4: 95 percent / 1 M LAH / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature

5: 99 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; dilithium tetrachlorocuprate; pyridinium p-toluenesulfonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00048a020