3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal

Base Information

Chemical Name:3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal
CAS No.:127540-48-1
Molecular Formula:C₁₁H₂₂O₄
Molecular Weight:218.293
Hs Code.:

Synonyms:3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal

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Technology Process of 3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal

There total 2 articles about 3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 6314-88-1
1,2,5,6-tetrahydrobenzaldehyde diethyl acetal

: 127540-48-1
3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; for 2h;
DOI:10.1021/jm00169a023

Reference yield:

: 100-50-5,61746-36-9
3-Cyclohexene-1-carboxaldehyde

: 127540-48-1
3,4-dihydroxycyclohexanecarboxaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Amberlyst 15 / 1 h / 4 °C

2: 73 percent / N-methylmorpholine N-oxide, OsO₄ / H₂O; tetrahydrofuran / 2 h

With osmium(VIII) oxide; Amberlyst 15; 4-methylmorpholine N-oxide; In tetrahydrofuran; water;
DOI:10.1021/jm00169a023