(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H⁽¹⁺⁾*O₃SC₆H₄CH₃^(1-)={(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H}{O₃SC₆H₄CH₃}

Base Information

• Chemical Name: (C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H⁽¹⁺⁾*O₃SC₆H₄CH₃^(1-)={(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H}{O₃SC₆H₄CH₃}
• CAS No.: 96213-74-0
• Molecular Formula: C₇H₇O₃S*C₃₅H₃₁NOP₂Re
• Molecular Weight: 900.989

Synonyms:(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H⁽¹⁺⁾*O₃SC₆H₄CH₃^(1-)={(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H}{O₃SC₆H₄CH₃}

Chemical Property of (C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H⁽¹⁺⁾*O₃SC₆H₄CH₃^(1-)={(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H}{O₃SC₆H₄CH₃}

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Technology Process of (C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H⁽¹⁺⁾*O₃SC₆H₄CH₃^(1-)={(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H}{O₃SC₆H₄CH₃}

There total 1 articles about (C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H⁽¹⁺⁾*O₃SC₆H₄CH₃^(1-)={(C₅H₅)Re(NO)(P(C₆H₅)3)P(C₆H₅)2H}{O₃SC₆H₄CH₃} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(C5H5)Re(NO)(P(C6H5)3)O3SC6H4CH3 (92695-37-9) + diphenylphosphane (829-85-6) → (C5H5)Re(NO)(P(C6H5)3)P(C6H5)2H(1+)*O3SC6H4CH3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C6H5)2H}{O3SC6H4CH3} (96213-74-0)

Guidance literature:

In dichloromethane; (C5H5)Re(NO)PpO3SC6H4CH3 and PPh2H stirred in CH2Cl2 for 2 d; soln. concd. in vacuo and added to ether; formed ppt. filtered, washed with ether, air-dried, recrystallized from CHCl3/ether and dried in vacuo; elem. anal.;

DOI:10.1021/ja00216a015

Reference yield: 99.0%

(C5H5)Re(NO)(P(C6H5)3)P(C6H5)2H(1+)*O3SC6H4CH3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C6H5)2H}{O3SC6H4CH3} (96213-74-0) + potassium tert-butylate (865-47-4) → (η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2 (96213-75-1)

Guidance literature:

In tetrahydrofuran; {(C5H5)Re(NO)PpPPh2H}{O3SC6H4CH3} and K{C(CH3)3O} stirred in THF for 3 h; mixture filtered; filtrate concd.; after addn. of ether formed ppt. filtered, washed with ether and dried in vacuo; (C5H5)Re(NO)PpPPh2 recrystd. from THF/hexane and dried in vacuo at 56 ° C; elem. anal.;

DOI:10.1021/ja00216a015

Reference yield: 97.0%

(C5H5)Re(NO)(P(C6H5)3)P(C6H5)2H(1+)*O3SC6H4CH3(1-)={(C5H5)Re(NO)(P(C6H5)3)P(C6H5)2H}{O3SC6H4CH3} (96213-74-0) → (η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2 (96213-75-1)

Guidance literature:

With t-C₄H₉OK; In not given; elem. anal.;

DOI:10.1021/ja00297a050

upstream raw materials:

(C₅H₅)Re(NO)(P(C₆H₅)3)O₃SC₆H₄CH₃

diphenylphosphane

Downstream raw materials:

(η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2

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