cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester

Base Information

• Chemical Name: cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester
• CAS No.: 950665-60-8
• Molecular Formula: C₃₈H₅₆O₇
• Molecular Weight: 624.858

Synonyms:cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester

Chemical Property of cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester

Chemical Property:

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Technology Process of cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester

There total 2 articles about cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

enoxolone (471-53-4) + cis-1,2-cyclohexane dicarboxylic anhydride → cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester + cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester (950665-60-8)

Guidance literature:

enoxolone; cis-1,2-cyclohexane dicarboxylic anhydride; With pyridine; dmap; at 100 ℃; for 16 - 20h;

With hydrogenchloride; water;

Reference yield:

→ cis-cyclohexane-1,2-dicarboxylic acid mono-((3S,4aR,6aR,6bS,8aS,11S,12aR,14aR,14bS)-11-carboxy-4,4,6a,6b,8a,11,14b-heptamethyl-14-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-icosahydro-picen-3yl) ester (950665-60-8)

Guidance literature:

18β-Glycyrrhetinsaeure, cis-Cyclohexan-1,2-dicarbonsaeureanhydrid, Pyridin;

upstream raw materials:

enoxolone

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