Technology Process of trans-3-acrylsaeure-methylester
There total 7 articles about trans-3-acrylsaeure-methylester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine;
In
diethyl ether;
for 20h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: ethyl acetate / 0.5 h / Ambient temperature
2: 35 percent H2O2 / ethyl acetate; tetrahydrofuran / 1 h / Ambient temperature
3: 72 percent / LiAlH4 / diethyl ether / 1 h / Ambient temperature
4: 83 percent / tert-butylhydroperoxide, VO(acac)2 / benzene / 48 h / 40 °C
5: 99 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature
6: 66 percent / hydrazin hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature
7: 88 percent / 4-methylmorpholine / diethyl ether / 20 h / Ambient temperature
With
4-methyl-morpholine; pyridine; chromium(VI) oxide; tert.-butylhydroperoxide; lithium aluminium tetrahydride; bis(acetylacetonate)oxovanadium; dihydrogen peroxide; hydrazine hydrate; acetic acid;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; ethyl acetate; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature
2: 66 percent / hydrazin hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature
3: 88 percent / 4-methylmorpholine / diethyl ether / 20 h / Ambient temperature
With
4-methyl-morpholine; pyridine; chromium(VI) oxide; hydrazine hydrate; acetic acid;
In
diethyl ether; ethanol; dichloromethane;
