ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

Base Information

Chemical Name:ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate
CAS No.:121099-87-4
Molecular Formula:C₂₄H₃₀ClFO₃
Molecular Weight:420.952
Hs Code.:

Synonyms:ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

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Chemical Property of ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

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Technology Process of ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

There total 4 articles about ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 121099-60-3
ethyl 7-(4-fluorophenyl)-7-(2-hydroxy-3,4,6-trimethylphenyl)heptanoate

: 121099-87-4
ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

Guidance literature:: With sulfuryl dichloride; for 1h; Ambient temperature;
DOI:10.1021/jm00090a009

Reference yield:

: 121099-61-4
7-(4-fluorophenyl)-7-(2-hydroxy-3,4,6-trimethylphenyl)heptanoic acid

: 121099-87-4
ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

Guidance literature:: With sulfuryl dichloride; In ice-water; sodium hydrogencarbonate;

Reference yield:

: 697-82-5
2,3,5-trimethylphenol

: 121099-87-4
ethyl 7-(5-chloro-2-hydroxy-3,4,6-trimethylphenyl)-7-(4-fluorophenyl)heptanoate

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*Et₂O / 1,2-dichloro-ethane / 6 h / 60 °C

2: 92 percent / SO₂Cl₂ / 1 h / Ambient temperature

With sulfuryl dichloride; boron trifluoride diethyl etherate; In 1,2-dichloro-ethane;
DOI:10.1021/jm00090a009