3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

Base Information

Chemical Name:3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate
CAS No.:1449038-88-3
Molecular Formula:C₂₀H₂₁ClN₂O₄S
Molecular Weight:420.917
Hs Code.:

Synonyms:3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

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Chemical Property of 3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

Chemical Property:

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Technology Process of 3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

There total 3 articles about 3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1449038-86-1
3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propan-1-ol

: 98-59-9
p-toluenesulfonyl chloride

: 1449038-88-3
3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

Guidance literature:: 3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propan-1-ol; With potassium hydroxide; at 20 ℃; for 0.0833333h;

p-toluenesulfonyl chloride; With potassium carbonate; at 20 ℃; for 0.333333h;
DOI:10.1016/j.ejmech.2013.05.027

Reference yield:

: 63874-99-7
1-(4-chlorophenyl)-1H-pyrazole-4-carbaldehyde

: 1449038-88-3
3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 0.25 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2.2: 4 h / 0 °C

3.1: borane-THF / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Darkness

3.2: 12 h / 20 °C / Inert atmosphere

4.1: potassium hydroxide / 0.08 h / 20 °C

4.2: 0.33 h / 20 °C

With sodium tetrahydroborate; borane-THF; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.ejmech.2013.05.027

Reference yield:

: 851180-84-2
(1-(4-chlorophenyl)-1H-pyrazol-4-yl)methanol

: 1449038-88-3
3-((1-(4-chlorophenyl)-1H-pyrazol-4-yl)methoxy)propyl 4-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

1.2: 4 h / 0 °C

2.1: borane-THF / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Darkness

2.2: 12 h / 20 °C / Inert atmosphere

3.1: potassium hydroxide / 0.08 h / 20 °C

3.2: 0.33 h / 20 °C

With borane-THF; sodium hydride; potassium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2013.05.027