(E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine

Base Information

• Chemical Name: (E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine
• CAS No.: 1361966-86-0
• Molecular Formula: C₂₄H₃₂BNO₃
• Molecular Weight: 393.334

Synonyms:(E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine

Chemical Property of (E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine

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Technology Process of (E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine

There total 1 articles about (E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-((3E)-4-(4-methoxyphenyl)but-3-en-2-ylidene)-1-phenylmethanamine + bis(pinacol)diborane (73183-34-3) → (E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine (1361966-86-0)

Guidance literature:

bis(pinacol)diborane; With triphenylphosphine; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; for 0.0833333h; Inert atmosphere;

N-((3E)-4-(4-methoxyphenyl)but-3-en-2-ylidene)-1-phenylmethanamine; With methanol; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1002/chem.201102081

Reference yield: 80.0%

(E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine (1361966-86-0) → 3-(benzylamino)-1-(4-methoxyphenyl)butan-1-ol + 3-(benzylamino)-1-(4-methoxyphenyl)butan-1-ol

Guidance literature:

(E)-N-(4-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-ylidene)-1-phenylmethanamine; With borane-THF; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 3h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;

DOI:10.1002/chem.201102081

upstream raw materials:

bis(pinacol)diborane

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