C₁₅H₂₂N₂O₄

Base Information

• Chemical Name: C₁₅H₂₂N₂O₄
• CAS No.: 1318779-85-9
• Molecular Formula: C₁₅H₂₂N₂O₄
• Molecular Weight: 294.351
• Mol file: 1318779-85-9.mol

Synonyms:C₁₅H₂₂N₂O₄

Chemical Property of C₁₅H₂₂N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₂N₂O₄

There total 1 articles about C₁₅H₂₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-((2-ethylhexyl)oxy)-5-nitrobenzoic acid (1039902-87-8) → C15H22N2O4 (1318779-85-9)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C / Reflux

2: ammonium hydroxide

With ammonium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;

DOI:10.1021/ol2018455

Reference yield: 99.0%

C15H22N2O4 (1318779-85-9) + benzoyl chloride (98-88-4) → C22H26N2O5 (1318779-87-1)

Guidance literature:

C₁₅H₂₂N₂O₄; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

benzoyl chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1021/ol2018455

Reference yield:

C15H22N2O4 (1318779-85-9) → C30H32F3N3O4 (1318779-79-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 0.08 h / 20 °C

2.1: 14% Pd/C; hydrogen / dichloromethane / 20 °C

3.1: dichloromethane / 5 h / 20 °C / Inert atmosphere

With 14% Pd/C; hydrogen; sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol2018455

upstream raw materials:

2-((2-ethylhexyl)oxy)-5-nitrobenzoic acid

Downstream raw materials:

C₃₀H₃₂F₃N₃O₄

C₂₂H₂₈N₂O₃

C₂₂H₂₆N₂O₅