(2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one

Base Information

• Chemical Name: (2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one
• CAS No.: 133868-42-5
• Molecular Formula: C₂₄H₂₈O₄
• Molecular Weight: 380.484

Synonyms:(2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one

Chemical Property of (2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one

Chemical Property:

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Technology Process of (2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one

There total 2 articles about (2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) + (C6H11)CHOCO2Si(CH3)3C3H4(C6H5) (116279-22-2) → (2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one (133868-42-5) + (2R,5R)-2-((1S,2S)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one (121097-26-5,133868-42-5)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 6h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/ja00194a061

Reference yield:

benzaldehyde (100-52-7) + (C6H11)CHOCO2Si(CH3)3C3H4(C6H5) (116279-22-2) → (2R,5R)-2-((1R,2R)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one (133868-42-5) + (2R,5R)-2-((1S,2S)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one (121097-26-5,133868-42-5)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 6h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/ja00194a061

Reference yield:

(2R,5R)-2-((1S,2S)-1-Benzyl-2-hydroxy-2-phenyl-ethyl)-5-cyclohexyl-[1,3]dioxolan-4-one (121097-26-5,133868-42-5) → (R)-2-Benzyl-1-phenyl-propane-1,3-diol (121097-35-6,121097-42-5) + (R)-2-Benzyl-1-phenyl-propane-1,3-diol (121097-35-6,121097-42-5)

Guidance literature:

With lithium aluminium tetrahydride; Title compound not separated from byproducts;

DOI:10.1021/ja00194a061

upstream raw materials:

benzaldehyde

(C₆H₁₁)CHOCO₂Si(CH₃)3C₃H₄(C₆H₅)

Downstream raw materials:

(R)-2-Benzyl-1-phenyl-propane-1,3-diol

(R)-2-Benzyl-1-phenyl-propane-1,3-diol

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