2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

Base Information

Chemical Name:2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose
CAS No.:152453-72-0
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

Synonyms:2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

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Chemical Property of 2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

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Technology Process of 2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

There total 8 articles about 2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 152453-71-9
(1'S,4R)-4-(3',3'-bisethylthio-1'-p-methoxybenzyloxypropyl)-2,2-dimethyl-1,3-dioxolane

: 152453-72-0
2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetonitrile;
DOI:10.1016/S0040-4039(00)01285-5

Reference yield:

: 1287289-41-1
C₁₇H₂₆O₆

: 152453-72-0
2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

Guidance literature:: With lead(IV) tetraacetate; In toluene; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2016.09.041

Reference yield:

: 67320-20-1,83692-41-5,94292-91-8,64722-95-8
1-(2,2-dimethyl-[1,3]dioxolan-4-yl)-3,3-bis-ethylsulfanyl-propan-1-ol

: 152453-72-0
2-deoxy-3-O-<(4-methoxyphenyl)methyl>-4,5-O-(1-methylethylidene)-D-erythro-pentose

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / sodium hydride / dimethylformamide; various solvent(s) / 2 h

2: 85 percent / HgCl₂; yellow HgO / acetonitrile; H₂O / 0.67 h / 0 °C

With sodium hydride; mercury dichloride; mercury(II) oxide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)00279-4