4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester

Base Information

• Chemical Name: 4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester
• CAS No.: 79727-61-0
• Molecular Formula: C₂₆H₃₃ClO₃
• Molecular Weight: 428.999

Synonyms:4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester

Chemical Property of 4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester

Chemical Property:

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Technology Process of 4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester

There total 2 articles about 4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

1-[4-(3,7-Dimethyl-oct-6-enyloxy)-phenyl]-propan-1-ol (79727-53-0) + 4-chloro-benzoyl chloride (122-01-0) → 4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester (79727-61-0)

Guidance literature:

In pyridine; Ambient temperature;

DOI:10.1135/cccc19811614

Reference yield:

4-(3,7-dimethyl-2-octenyloxy)propiophenone (79728-06-6) → 4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester (79727-61-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

2: 46 percent / pyridine / Ambient temperature

With lithium aluminium tetrahydride; In pyridine; diethyl ether;

DOI:10.1135/cccc19811614

Reference yield: 37.0%

4-Chloro-benzoic acid 1-[4-(3,7-dimethyl-oct-6-enyloxy)-phenyl]-propyl ester (79727-61-0) → 4-Chloro-benzoic acid 1-{4-[5-(3,3-dimethyl-oxiranyl)-3-methyl-pentyloxy]-phenyl}-propyl ester (79727-77-8)

Guidance literature:

With monoperoxyphthalic acid; In diethyl ether; at 10 - 20 ℃; for 0.5h;

DOI:10.1135/cccc19811614

upstream raw materials:

1-[4-(3,7-Dimethyl-oct-6-enyloxy)-phenyl]-propan-1-ol

4-chloro-benzoyl chloride

4-(3,7-dimethyl-2-octenyloxy)propiophenone

Downstream raw materials:

4-Chloro-benzoic acid 1-{4-[5-(3,3-dimethyl-oxiranyl)-3-methyl-pentyloxy]-phenyl}-propyl ester

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