methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate

Base Information

• Chemical Name: methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate
• CAS No.: 641614-05-3
• Molecular Formula: C₂₈H₄₀O₃
• Molecular Weight: 424.624

Synonyms:methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate

Chemical Property of methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate

Chemical Property:

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Technology Process of methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate

There total 2 articles about methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-geranyl bromide (6138-90-5) → methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate (641614-05-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / NaOH

2: 91 percent / Et₃N / Cl₂Pd(PPh₃)2 / dimethylformamide / 6 h / 60 °C / 760 Torr

With sodium hydroxide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide;

DOI:10.1271/bbb.67.2038

Reference yield:

p-Iodophenol (540-38-5) → methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate (641614-05-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / NaOH

2: 91 percent / Et₃N / Cl₂Pd(PPh₃)2 / dimethylformamide / 6 h / 60 °C / 760 Torr

With sodium hydroxide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide;

DOI:10.1271/bbb.67.2038

Reference yield: 88.0%

methyl (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoate (641614-05-3) → (2'E,2''E)-4-hydroxy-3-(3',7'-dimethylocta-2',6'-dienyl)-5-(3'',7''-dimethylocta-2'',6''-dienyl)benzoic acid

Guidance literature:

With sodium hydroxide; In methanol; Heating;

DOI:10.1271/bbb.67.2038

upstream raw materials:

trans-geranyl bromide

p-Iodophenol

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