Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

Base Information

Chemical Name:Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin
CAS No.:1358953-91-9
Molecular Formula:C₆₀H₅₆Br₄N₄Zn
Molecular Weight:1218.14
Hs Code.:

Synonyms:Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

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Chemical Property of Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

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Technology Process of Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

There total 2 articles about Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 7,8,17,18-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

: 557-34-6
zinc diacetate

: 1358953-91-9
Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

Guidance literature:: In methanol; dichloromethane; at 50 ℃; for 3.5h;
DOI:10.1039/c5ta07226c

Reference yield:

: 110452-48-7
5,10,15,20-tetrakis(p-tert-butylphenyl)porphyrin

: 1358953-91-9
Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; pyridine / chloroform / 11.25 h / 80 °C

2: dichloromethane; methanol / 3.5 h / 50 °C

With pyridine; N-Bromosuccinimide; In methanol; dichloromethane; chloroform;
DOI:10.1039/c5ta07226c

Reference yield: 56.0%

: 557-21-1
zinc(II) cyanide

: 1358953-91-9
Zn(II) 2,3,12,13-tetrabromo-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

: Zn(II) 2,3,12,13-tetracyano-5,10,15,20-tetrakis-(4-t-butylphenyl)porphyrin

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc; In N,N-dimethyl acetamide; at 115 ℃; for 27h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c5ta07226c