dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

Base Information

Chemical Name:dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate
CAS No.:889686-18-4
Molecular Formula:C₂₂H₂₈NO₃P
Molecular Weight:385.443
Hs Code.:

Synonyms:dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

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Chemical Property of dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

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Technology Process of dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

There total 3 articles about dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 889686-11-7
dimethyl (2E)-1-(allylamino)-2-methyl-3-phenylprop-2-enylphosphonate

: 100-39-0
benzyl bromide

: 889686-18-4
dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

Guidance literature:: With potassium carbonate; sodium iodide; In acetone; Heating;
DOI:10.1021/jo060160e

Reference yield:

: 118673-08-8
Allyl-[(E)-2-methyl-3-phenyl-prop-2-en-(E)-ylidene]-amine

: 889686-18-4
dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / methanol / Heating

2: 50 percent / K₂CO₃; NaI / acetone / Heating

With potassium carbonate; sodium iodide; In methanol; acetone;
DOI:10.1021/jo060160e

Reference yield:

: 15174-47-7
α-methyl-trans-cinnamaldehyde

: 889686-18-4
dimethyl (2E)-1-(allyl(benzyl)amino)-2-methyl-3-phenylprop-2-enylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: MgSO₄ / CH₂Cl₂ / 20 °C

2: 90 percent / methanol / Heating

3: 50 percent / K₂CO₃; NaI / acetone / Heating

With magnesium sulfate; potassium carbonate; sodium iodide; In methanol; dichloromethane; acetone;
DOI:10.1021/jo060160e