3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Base Information

Chemical Name:3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide
CAS No.:299924-42-8
Molecular Formula:C₂₁H₁₉O₂PS
Molecular Weight:366.42
Hs Code.:

Synonyms:3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Suppliers and Price of 3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

There total 6 articles about 3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 299924-39-3
4,5-dimethyl-2-methoxycarbonyl-3,6-diphenyl-1-phospha-2,5-norbornadiene sulfide

: 299924-42-8
3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Guidance literature:: With lithium iodide; In pyridine; at 150 ℃; for 20h;
DOI:10.1021/ol006323h

Reference yield:

: 299924-64-4
4,5-dimethyl-2-pethoxycarbonyl-3,6-diphenyl-1-phospha-2,5-norbornadiene sulfide

: 299924-42-8
3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; ethanol; water; at 0 - 20 ℃; for 15h;
DOI:10.1021/ol006323h

Reference yield:

: 299924-63-3
4,5-dimethyl-2-methoxycarbonyl-3,6-diphenyl-1-phospha-2,5-norbornadiene

: 299924-42-8
3,6-diphenyl-4,5-dimethyl-2-hydroxycarbonyl-1-phospha-2,5-norbornadiene sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / S₈ / toluene / 12 h / 90 - 95 °C

2: LiI / pyridine / 20 h / 150 °C

With sulfur; lithium iodide; In pyridine; toluene; 1: Oxidation / 2: Hydrolysis;
DOI:10.1021/ol006323h