2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

Base Information

Chemical Name:2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol
CAS No.:198775-36-9
Molecular Formula:C₃₂H₂₈N₂O₈
Molecular Weight:568.583
Hs Code.:

Synonyms:2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

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Chemical Property of 2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

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Technology Process of 2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

There total 8 articles about 2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 77890-04-1
2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-ribo-hexitol

: 4330-20-5
N-3-benzoylthymine

: 198775-36-9
2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In acetonitrile; Inert atmosphere;
DOI:10.1080/15257770903306518

Reference yield:

: 37699-02-8,94273-27-5,94283-95-1,122194-15-4
(3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

: 198775-36-9
2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

Guidance literature:: Multi-step reaction with 7 steps

1: NaBH₄

2: H₂ / Pd/C

3: HClO₄

4: pyridine

5: H₂SO₄ / methanol

6: 1.) (Im)2CS, 2.) Bu₃SnH, AIBN / 1.) DMF, 2.) toluene, reflux

7: 67 percent / PPh₃, DEAD / dioxane

With sodium tetrahydroborate; perchloric acid; 2,2'-azobis(isobutyronitrile); sulfuric acid; hydrogen; tri-n-butyl-tin hydride; 1,1'-Thiocarbonyldiimidazole; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In 1,4-dioxane; pyridine; methanol;
DOI:10.1080/07328319708006130

Reference yield:

: 198775-13-2
((3R,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-methanol

: 198775-36-9
2,5-anhydro-4,6-di-O-benzoyl-1-(N-3-benzoylthymin-1-yl)-3-deoxy-D-ribo-hexitol

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / Pd/C

2: HClO₄

3: pyridine

4: H₂SO₄ / methanol

5: 1.) (Im)2CS, 2.) Bu₃SnH, AIBN / 1.) DMF, 2.) toluene, reflux

6: 67 percent / PPh₃, DEAD / dioxane

With perchloric acid; 2,2'-azobis(isobutyronitrile); sulfuric acid; hydrogen; tri-n-butyl-tin hydride; 1,1'-Thiocarbonyldiimidazole; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In 1,4-dioxane; pyridine; methanol;
DOI:10.1080/07328319708006130