salicylaldehyde-N,N-diphenyl semicarbazone

Base Information

Chemical Name:salicylaldehyde-N,N-diphenyl semicarbazone
CAS No.:29416-53-3
Molecular Formula:C₂₀H₁₇N₃O₂
Molecular Weight:331.374
Hs Code.:

Synonyms:salicylaldehyde-N,N-diphenyl semicarbazone

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Chemical Property of salicylaldehyde-N,N-diphenyl semicarbazone

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Technology Process of salicylaldehyde-N,N-diphenyl semicarbazone

There total 4 articles about salicylaldehyde-N,N-diphenyl semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-02-8
salicylaldehyde

: 603-51-0
N,N-diphenyl semicarbazide

: 29416-53-3
salicylaldehyde-N,N-diphenyl semicarbazone

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.jinorgbio.2012.10.011

Reference yield:

: 83-01-2
diphenylcarbamic chloride

: 29416-53-3
salicylaldehyde-N,N-diphenyl semicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / diethyl ether; ethanol / 0.5 h / Schlenk technique; Inert atmosphere

2: toluene-4-sulfonic acid / toluene / 0.5 h / 20 °C / Schlenk technique; Inert atmosphere

With toluene-4-sulfonic acid; hydrazine hydrate; In diethyl ether; ethanol; toluene;
DOI:10.1016/j.jinorgbio.2012.10.011

Reference yield:

: 122-39-4
diphenylamine

: 29416-53-3
salicylaldehyde-N,N-diphenyl semicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / Cooling with ice; Schlenk technique; Inert atmosphere

2: hydrazine hydrate / diethyl ether; ethanol / 0.5 h / Schlenk technique; Inert atmosphere

3: toluene-4-sulfonic acid / toluene / 0.5 h / 20 °C / Schlenk technique; Inert atmosphere

With pyridine; toluene-4-sulfonic acid; hydrazine hydrate; In diethyl ether; ethanol; dichloromethane; toluene;
DOI:10.1016/j.jinorgbio.2012.10.011