(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

Base Information

Chemical Name:(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside
CAS No.:1356821-80-1
Molecular Formula:C₃₃H₃₅ClN₄O₈S
Molecular Weight:683.182
Hs Code.:

Synonyms:(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

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Chemical Property of (3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

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Technology Process of (3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

There total 9 articles about (3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1356821-79-8
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

: 1356821-80-1
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

Guidance literature:: With acetic acid; at 40 ℃;
DOI:10.1016/j.ejmech.2011.10.028

Reference yield:

: 1356821-73-2
allyl 2,3-O-cyclopentylidene-5-deoxy-5-azide-β-D-ribofuranoside

: 1356821-80-1
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 7 steps

1: triphenylphosphine / 1,4-dioxane / 24 h / 20 °C / Inert atmosphere

2: 1,4-dioxane / 24 h / 20 °C / Inert atmosphere

3: sodium ethanolate / ethanol / 24 h / Reflux

4: acetic acid / 24 h / 40 °C

5: potassium carbonate / acetone / 17 h / 20 °C

6: chloroamine-T / water; tert-butyl alcohol / 5 h / 20 °C

7: acetic acid / 40 °C

With sodium ethanolate; chloroamine-T; potassium carbonate; acetic acid; triphenylphosphine; In 1,4-dioxane; ethanol; water; acetone; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2011.10.028

Reference yield:

: 1356821-75-4
allyl 5-(p-chlorobenzohydrazidocarbothionyl)amino-2,3-O-cyclopentylidene-5-deoxy-β-D-ribofuranoside

: 1356821-80-1
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: sodium ethanolate / ethanol / 24 h / Reflux

2: acetic acid / 24 h / 40 °C

3: potassium carbonate / acetone / 17 h / 20 °C

4: chloroamine-T / water; tert-butyl alcohol / 5 h / 20 °C

5: acetic acid / 40 °C

With sodium ethanolate; chloroamine-T; potassium carbonate; acetic acid; In ethanol; water; acetone; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2011.10.028